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<li class="p_navItem1"> <p class="p_navCon js_editor_click"> <a href="/Brand_list/1203994689079033856.html" target="" > <span>鍝佺墝椋庨噰</span> </a> <svg t="1638932461478" class="icon p_jtIcon" viewBox="0 0 1024 1024" version="1.1" xmlns="http://www.w3.org/2000/svg" p-id="2646" width="16" height="16"><path d="M761.055557 532.128047c0.512619-0.992555 1.343475-1.823411 1.792447-2.848649 8.800538-18.304636 5.919204-40.703346-9.664077-55.424808L399.935923 139.743798c-19.264507-18.208305-49.631179-17.344765-67.872168 1.888778-18.208305 19.264507-17.375729 49.631179 1.888778 67.872168l316.960409 299.839269L335.199677 813.631716c-19.071845 18.399247-19.648112 48.767639-1.247144 67.872168 9.407768 9.791372 21.984142 14.688778 34.560516 14.688778 12.000108 0 24.000215-4.479398 33.311652-13.439914l350.048434-337.375729c0.672598-0.672598 0.927187-1.599785 1.599785-2.303346 0.512619-0.479935 1.056202-0.832576 1.567101-1.343475C757.759656 538.879828 759.199462 535.391265 761.055557 532.128047z" 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0.927187-1.599785 1.599785-2.303346 0.512619-0.479935 1.056202-0.832576 1.567101-1.343475C757.759656 538.879828 759.199462 535.391265 761.055557 532.128047z" p-id="2647"></path></svg> </a> <svg t="1638932461478" class="icon p_jtIcon" viewBox="0 0 1024 1024" version="1.1" xmlns="http://www.w3.org/2000/svg" p-id="2646" width="16" height="16"><path d="M761.055557 532.128047c0.512619-0.992555 1.343475-1.823411 1.792447-2.848649 8.800538-18.304636 5.919204-40.703346-9.664077-55.424808L399.935923 139.743798c-19.264507-18.208305-49.631179-17.344765-67.872168 1.888778-18.208305 19.264507-17.375729 49.631179 1.888778 67.872168l316.960409 299.839269L335.199677 813.631716c-19.071845 18.399247-19.648112 48.767639-1.247144 67.872168 9.407768 9.791372 21.984142 14.688778 34.560516 14.688778 12.000108 0 24.000215-4.479398 33.311652-13.439914l350.048434-337.375729c0.672598-0.672598 0.927187-1.599785 1.599785-2.303346 0.512619-0.479935 1.056202-0.832576 1.567101-1.343475C757.759656 538.879828 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href="/Academic_details/1203993859164684288.html" target="_self"> 娓呴櫎鍐呴暅娈嬬暀閭昏嫰浜岀敳閱涙柟妗堢殑鎺㈣ </a> </p><p class="e_text-15 s_title"> 閭昏嫰浜岀敳閱? Orthophthalaldehyde锛孫PA) 鐢变簬鍏鍒烘縺鎬ф皵鍛冲皬銆佹秷姣掓椂闂寸煭鐨勪紭鐐逛綔涓虹浜屼唬鍐呴暅娓呮礂娑堟瘨鍓傝繎骞存潵閫愭笎琚箍娉涘簲鐢紝鐜伴樁娈垫棩鏈偦鑻簩鐢查啗鐨勪娇鐢ㄧ巼涓 45% 锛岀編鍥戒负 41%銆?銆曘€備絾鐢变簬鍏舵槗鑷存晱鍙嶅簲琚鐢ㄤ簬鑶€鑳遍暅娑堟瘨锛屼笖娈嬬暀 OPA 浼瀵规偅鑰呰儍鑲犻粡鑶滀骇鐢熸崯瀹炽€?銆曪紝瀵艰嚧寮備笝閱囦紤鍏嬪弽搴斻€?銆曘€傝櫧鐒剁幇鏈夌殑鍥藉唴澶栧唴闀滄寚鍗楀潎寮鸿皟浜嗘竻娲姝ラ瀵规畫鐣欐秷姣掑墏鐨勬竻闄や綔鐢ㄣ€?銆曪紝浣嗗浜庡疄闄呭唴闀鐨 OPA 娈嬬暀閲忓強鏈夋晥娓呴櫎鏂规硶鏆傛棤鐩稿叧鐮旂┒鎶ラ亾銆鍥犳锛屾湰鐮旂┒浠庡姘村钩澶勭悊鏂规楠岃瘉 OPA 缁忎笉鍚屾竻娲楁椂闂村拰鏂规硶鍚庣殑娈嬬暀閲忥紝浠ユ湡涓轰复搴婅鑼冨埗瀹氬拰搴旂敤鎻愪緵鐞嗚渚濇嵁鏉愭枡涓庢柟娉 1锛 1 璇曢獙鏉愭枡楂樻晥娑茬浉鑹茶氨浠紝1200 HPLC( Agilent technolo?gies 鍏徃) ; 婕╂丁鎸崱鍣? SL 锛 A256( Scientific Indus?tries 鍏徃) ; 2锛? 锛浜岀鍩鸿嫰鑲机鍚噺 99% ( 骞垮窞鍖栧 路 2611 路 Chinese Journal of Disinfection 2016; 33( 12)璇曞墏鍘? ; 涔欒厛: 鑹茶氨绾? ME锛睰鍏徃) ; 閭昏嫰浜岀敳閱汑鍚噺 99% ( SIGMA 锛 ALD锛睮CH 鍏徃) 銆鏈爺绌堕噰鐢ㄧ殑鍐呴暅涓 GIF 锛 Q260J( Olympus 鍏鍙? 锛?锛 55% CIDEX顡 OPA 娑堟瘨娑? 寮虹敓鍏徃) 锛屼竴浣鍖栧唴闀滄竻娲楁秷姣掓按妲 1 濂? 娣卞湷鏌附灏? 锛岃嚜鍔ㄥ柗娣寮忓唴绐ラ暅娓呮礂娑堟瘨妲 1 濂? 鍥藉瀹炵敤鏂板瀷涓撳埄: ZL 2013 2 0185558锛 2) 锛屽唴闀滆嚜鍔ㄦ竻娲楁秷姣掓満 1 鍙? 寮鐢熷叕鍙? 銆 1锛 2 璇曢獙鏂规硶 1锛 2锛 1 鍒嗙粍鏂规硶璇曢獙鍒嗕负 4 缁凓绗 1 缁勪负绌虹櫧瀵圭収缁勶紝鐩存帴浣跨敤杩囨护姘存竻娲楀悗閲囨牱; 绗 2 缁勪负鍗曡偂姘娴佺粍锛岄噰鐢ㄤ紶缁熸按榫欏ご杩涜娓呮礂; 绗 3 缁勪负鍠锋穻寮忔竻娲楃粍锛屼互娴侀噺姘存车涓轰緷鎵橈紝鍦ㄦ竻娲楁Ы妲戒綋鍚勫鍧囧畨瑁鏃嬭浆鍠锋穻澶达紝娓呮礂姘村彲浠庡柗娣嬪ご闆嗕腑灏勫嚭锛屽潎鍖€瑕嗙洊鍐叉礂鍐呴暅鎵€鏈夊琛ㄩ潰; 绗 4 缁勪负鑷姩娓呮礂娑堟瘨鏈虹粍锛浣跨敤鑷姩娓呮礂娑堟瘨鏈鸿繘琛屾竻娲椼€傞櫎绌虹櫧瀵圭収缁勫唴闀涓嶆蹈娉 OPA 澶栵紝瀹為獙缁勫唴闀滃潎鍏堟蹈娉 OPA 5 min銆姣忕粍鍚 12 鏉″唴闀滐紝娓呮礂鏃堕棿鍒嗕负 1銆?銆?銆? min 鍏 4 涓按骞炽€傛帶鍒惰繘姘寸鍘嬪姏锛屾瘡缁勬柟娉曟竻娲楁按閲忓潎涓 10 L /min銆 1锛 2锛 2 閲囨牱鏂规硶娓呮礂鍚庣殑鍐呴暅鐢ㄩ珮鍘嬫皵鏋惞骞诧紝灏嗙函鍖栨按娴告场鎻掑叆閮ㄥ琛ㄩ潰 5 min 鍚庢敹闆咞浣跨敤楂鏁堟恫鐩歌壊璋变华鍒嗘瀽娈嬬暀 OPA 娴撳害銆傚垎鍒綔鐢 1銆?銆 3銆? min銆 1锛 2锛 3 楂樻晥娑茬浉鑹茶氨娉鑹茶氨鍒嗘瀽 C18鑹茶氨鏌? 鍙閫夌敤 Lunna 锛 C18 鏌憋紝150mm 脳 4锛 6mm锛? ( m) 锛屾祦鍔鐩氟涔鑵圍姘 = 50: 50 ( v /v ) 锛屾煴娓? 25鈩冿紝娴閫烔 1 ml /min锛屾娴嬫尝闀菌 220 nm锛岃繘鏍蜂綋绉? 20 渭l銆 1锛 3 缁熻鏂规硶鏁版嵁浠 x鐝嬄 s 琛ㄧず锛岄噰鐢 SPSS 13锛 0 缁熻杞欢瀵鏁版嵁杩涜鍒嗘瀽锛岀敤澶氬洜绱犳瀽鍥犺璁℃柟宸垎鏋愬澶勭悊鏂规硶鍜屽鐞嗘椂闂翠綔缁熻鍒嗘瀽锛屽鍚屼竴缁勯棿涓嶅悓姘村钩鐨 OPA 娈嬬暀閲忛噰鐢 LSD 娉曡繘琛屾瘮杈冿紝P 锛 0锛 05 琛ㄧず宸紓鏈夌粺璁″鎰忎箟銆 2 缁撴灉搴旂敤鏋愬洜璁捐璧勬枡鏂瑰樊鍒嗘瀽涓嶅悓娓呮礂鏂规硶鍙婂 鐞嗘椂闂村悗 OPA 娈嬬暀閲忛棿宸紓锛屽潎瀛樺湪缁熻瀛﹀樊寮傦紝闇€閲囩敤 LSD 杩涜澶氶噸姣旇緝銆 2锛 1 涓嶅悓娓呮礂鏂规硶 OPA 娈嬬暀閲忕殑 LSD 澶氶噸姣旇緝鑷姩娓呮礂娑堟瘨鏈虹粍 OPA 娈嬬暀閲忔渶浣庯紝涓庣┖鐧藉 鐓х粍闂存棤缁熻瀛﹀樊寮傦紝娓呴櫎鏁堟灉鏈€浣炽€傚崟鑲℃按娴佺粍鐨 OPA 娈嬬暀閲忔渶楂橈紝涓庡悇缁勯棿鍧囧瓨鍦ㄦ樉钁楁€у樊寮傘€ 鍠锋穻寮忔竻娲楃粍涓庤嚜鍔ㄦ竻娲楁秷姣掓満缁勯棿鎴婁簩閱涙畫鐣欓噺铏芥棤缁熻瀛﹀樊寮傦紝浣嗗潎鍊兼瘮杈冨柗娣嬪紡娓呮礂缁勮緝鑷姩娓呮礂娑堟瘨鏈虹粍鍜岀┖鐧藉鐓х粍鍧囬珮( 琛 1) 銆琛 1 涓嶅悓娓呮礂鏂规硶瀵瑰唴闀滃琛ㄩ潰 OPA 娈嬬暀閲忓奖鍝嶇殑姣旇緝澶勭悊鏂规硶 ( I) 澶勭悊鏂规硶 ( J) MD ( I 锛 J) SE P 95% 缃俊鍖洪棿涓嬮檺涓婇檺绌虹櫧瀵圭収鍗曡偂姘存祦 -0锛 597* 0锛 085 0锛 000 -0锛 770 -0锛 423 鍠锋穻 -0锛 265* 0锛 085 0锛 004 -0锛 438 -0锛 092 鑷姩娲楁秷鏈 -0锛 127 0锛 085 0锛?44 -0锛 301 0锛 046 鍗曡偂姘存祦绌虹櫧瀵圭収 0锛 597* 0锛 085 0锛 000 0锛 423 0锛 770 鍠锋穻 0锛 332* 0锛 085 0锛 000 0锛 159 0锛 505 鑷姩娲楁秷鏈 0锛 469* 0锛 085 0锛 000 0锛 296 0锛 643 鍠锋穻绌虹櫧瀵圭収 0锛 265* 0锛 085 0锛 004 0锛 092 0锛 438 鍗曡偂姘存祦 -0锛 332* 0锛 085 0锛 000 -0锛 505 -0锛 159 鑷姩娲楁秷鏈 0锛 137 0锛 085 0锛 116 -0锛 036 0锛 311 鑷姩娲楁秷鏈绌虹櫧瀵圭収 0锛 127 0锛 085 0锛 144 -0锛 046 0锛 301 鍗曡偂姘存祦 -0锛 469* 0锛 085 0锛 000 -0锛 643 -0锛 296 鍠锋穻 -0锛 137 0锛 085 0锛 116 -0锛 311 0锛 036 娉? 鍩轰簬瑙傛祴鍒扮殑鍧囧€笺€? : 鍧囧€煎樊鍊煎湪 0锛 05 绾у埆涓婅緝鏄捐憲銆 2锛 2 涓嶅悓娓呮礂鏃堕棿 OPA 娈嬬暀閲忕殑 LSD 澶氶噸姣旇緝娓呮礂鏃堕棿涓 1 min 鏃讹紝OPA 鐨勬畫鐣欓噺涓庡叾浠栨椂闂寸偣鍏锋湁鏄捐憲鎬у樊寮傦紝2 min 涓 3 min銆? min 鏃堕棿缁闂存棤鏄捐憲鎬у樊寮傘€傚鐞嗘椂闂磋揪 2 min 鍚庡 OPA 鐨娈嬬暀閲忔竻闄ゆ晥鏋滄棤鍙樺寲( 琛 2) 銆琛 2 涓嶅悓娓呮礂鏃堕棿瀵瑰唴闀滃琛ㄩ潰 OPA 娈嬬暀閲忓奖鍝嶇殑姣旇緝澶勭悊鏃堕棿( min) ( I) 澶勭悊鏃堕棿( min) ( J) MD ( I 锛 J) SE P 95% 缃俊鍖洪棿涓嬮檺涓婇檺 1 2 0锛 300* 0锛 085 0锛 001 0锛 126 0锛 473 3 0锛 306* 0锛 085 0锛 001 0锛 133 0锛 479 4 0锛 258* 0锛 085 0锛 005 0锛 085 0锛 431 2 1 锛 0锛 300* 0锛 085 0锛 001 锛 0锛 473 锛 0锛 126 3 0锛 006 0锛 085 0锛 941 锛 0锛 167 0锛 180 4 锛 0锛 042 0锛 085 0锛 628 锛 0锛 215 0锛 132 3 1 锛 0锛 306* 0锛 0850锛 001 锛 0锛 479 锛 0锛 133 2 锛 0锛 006 0锛 085 0锛 941 锛 0锛 180 0锛 167 4 锛 0锛 048 0锛 085 0锛 576 锛 0锛 221 0锛 125 4 1 锛 0锛 258* 0锛 085 0锛 005 锛 0锛?31 锛 0锛 085 2 0锛 042 0锛 085 0锛 628 锛 0锛 132 0锛 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